Bruker pulse program two character code definitions
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For Bruker pulse programs the first characters (usually 4, but at a maximum 6) specify the type of experiment, e.g. DEPT, COSY, NOESY etc.. Further properties of the pulse program are indicated by a two-character code, which is added to the name in alphabetical order. For 2-D experiments the default version is “absolute value” and “without dummy scans”. H- or X-decoupling is assumed to be default for heteronuclear experiments, but not for homonuclear ones (with the exception of inad). In case of redundant information some two-character codes may be omitted.
The two-character codes used are the following:
bi with bird pulse for homonuclear J-decoupling
bp bipolar gradients
cp with composite pulse
ct constant time
cw decoupling using cw command
dc decoupling using cpd command
df double quantum filter
di with DIPSI mixing sequence
dh homonuclear decoupling in indirect dimension
dw decoupling using cpd command only during wet sequence
dq double quantum coherence
ea phase sensitive using Echo/Anti-echo method
ed with multiplicity editing
et phase sensitive using Echo/Anti-echo-TPPI method
fb using f2 - and f3 - channel
fd using f1 - and f3 - channel (for presaturation)
fr with presaturation using a frequency list
ft using f1 -, f2 - and f3 - channel (for presaturation)
fh F-19 observe with H-1 decoupling
fp a flip-back pulse
fl for F-19 decoupler
f2 using f2 - channel (for presaturation)
f3 using f3 - instead of f2 - channel
f4 using f4 - instead of f2 - channel
gd gated decoupling using cpd command
ge gradient echo experiment
gp coherence selection using gradients with “:gp” synthax
gr coherence selection using gradients
gs coherence selection using shaped gradients
hc homodecoupling of a region using a cpd-sequence
hd homodecoupling
hf H-1 observe with F-19 decoupling
hs with homospoil pulse
ig inverse gated
ii using inverse (invi/HSQC) sequence
im with incremented mixing time
i4 inverse (inv4/HMQC) sequence
jd homonuclear J-decoupled
jr with jump-return pulse
lp with low-pass J-filter
lq with Q-switching (low Q)
lr for long-range couplings
mf multiple quantum filter
ml with MLEV mixing sequence
nd no decoupling
no with NOESY mixing sequence
pc with presaturation and composite pulse
pg power-gated
pl preparing a frequency list
pn with presaturation using a 1-D NOESY sequence
pr with presaturation
ps with presaturation using a shaped pulse
qn for QNP-operation
qs phase sensitive using qseq-mode
rd refocused
rl with relay transfer
rs with radiation damping suppression using gradients
ru using radiation damping compensation unit
rv with random variation
r2 with 2 step relay transfer
r3 with 3 step relay transfer
se spin echo experiment
sh phase sensitive using States et al. method
si sensitivity improved
sm simultaneous evolution of X and Y chemical shift
sp a shaped pulse
st phase sensitive using States-TPPI method
sy symmetric sequence
tf triple quantum filter
tp phase sensitive using TPPI
tr using TROSY sequence
ul using a frequency list
us updating shapes
wg watergate using a soft-hard-soft sequence
w5 watergate using W5 pulse
xf x-filter experiments
x1 x-filter in F1
x2 x-filter in F2
zf with z-filter
zq zero quantum coherence
1d 1-D version
1s using 1 spoil gradients
11 using 1-1 pulse
19 using 3-9-19 pulse
2h using 2H lockswitch unit
2s using 2 spoil gradients
3d 3-D sequence
3s using 3 spoil gradients
30 using a 30 degree flip angle
45 using a 45 degree flip angle
90 using a 90 degree flip angle
135 using a 135 degree flip angle
A phase-sensitive (TPPI) NOESY experiment with presaturation would then be: noesy + pr + tp = noesyprtp.
文章作者 冯柳宾
上次更新 2019-06-17